HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | (2RS,3S)-3-amino-2-hydroxy-5-methylhexanoic acid | HCID 12879199 | — |
| Product | methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride | HCID 13746619 | — |
Reaction Steps
Hydrogen chloride was passed into a solution of 110 mg of (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoic acid in 10 ml of methanol with stirring, and the mixture was stirring overnight, and the mixture was evaporated to dryness under reduced pressure to obtain 150 mg of methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride as a white powder. [IR (KBr): νco 1740 cm-1 ].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04841067 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-9a387301a494401db47c6b1cae668875 |
| Source note | uspto-grants-1989_06 |