HRID1905333

反应详情

EQUATION

反应方程式

HRID 1905333 的结构方程式

PROCEDURE

实验过程

Hydrogen chloride was passed into a solution of 110 mg of (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoic acid in 10 ml of methanol with stirring, and the mixture was stirring overnight, and the mixture was evaporated to dryness under reduced pressure to obtain 150 mg of methyl (2RS, 3S)-3-amino-2-hydroxy-5-methylhexanoate hydrochloride as a white powder. [IR (KBr): νco 1740 cm-1 ].

WORKUP

后处理

  1. stirringthe mixture was stirring overnight
  2. customthe mixture was evaporated to dryness under reduced pressure