HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1905372Generated: October 31, 2026
Trimethyl phosphite → HCID 10397128, compound
https://huagongshe.com/reaction/1905372
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trimethyl phosphite | HCID 8472 | — |
| Reactant | 2,4-Pentanediol, (+)- | HCID 6950200 | — |
| Product | HCID 10397128 | HCID 10397128 | — |
Reaction Steps
10 g of (+)-(2S,4S)pentane-2,4-diol and 13.6 g of trimethylphosphite were mixed, and heated at 100° C. on an oil bath. After completion of distilling methanol off, the residue is distilled under reduced pressure to obtain colorless transparent 2-methoxy-(4S,6S)-4,6-dimethyl-1,3,2-dioxaphosphorinane. bp: 70°-72° C./15 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04843076 |
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| Source dataset | uspto-grants-1989_06 |
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| ORD ID | ord-82d308ee3d8b49a1be651a2daef599f0 |
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| Source note | uspto-grants-1989_06 |
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