HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoamyl Alcohol → HCID 14580252, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoamyl Alcohol | HCID 31260 | — |
| Reactant | 2-Pyridineacetic acid, hydrochloride (1:1) | HCID 85317 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14580252 | HCID 14580252 | — |
Reaction Steps
A mixture of 2-pyridylacetic acid hydrochloride 10.00 g (57.60 mmol), iso-amyl alcohol 6.09 g (69.12 mmol) and 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride 14.35 g (74.88 mmol) in 20 ml of pyridine and 80 ml of methylene chloride was stirred at room temperature for 2 hr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04843083 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-66b816e485f14bd7a565cd55e491db46 |
| Source note | uspto-grants-1989_06 |