Hydrochloric Acid → HCID 15631324, compound

Participants

Reaction Steps

A solution of 215.1 mg (0.85 mmol) of 5-benzoyl-1,2,3,4-tetrahydro-8-quinolinol in 5 ml of ether was treated with 3 ml of hydrogen chloride saturated ether. The fluffy white precipitate was filtered off and recrystallized from dichloromethane-methanol-hexane to obtain 130.8 mg of a white solid, dried at 56° C./0.1 mm of Hg; melting point 237°-239° C., dec.

Provenance & Evidence