HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-Decyl-1,2,3,4-tetrahydro-8-quinolinol, hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1-Decyl-1,2,3,4-tetrahydro-8-quinolinol | HCID 15631328 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-Decyl-1,2,3,4-tetrahydro-8-quinolinol, hydrochloride | HCID 15631329 | — |
Reaction Steps
A solution of 575.9 mg (1.99 mmol) of 1-decyl-1,2,3,4-tetrahydro-8-quinolinol in 1 ml of ether was treated with 5 ml of hydrogen chloride-saturated ether to afford a soluble hydrochloride. Evaporation provided an oil which solidified upon standing to give 564.2 mg of a waxy, ivory-colored solid:melting point 82°-83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04843082 |
| Source dataset | uspto-grants-1989_06 |
| ORD ID | ord-a8f52b5a9aa54019941eb20543477382 |
| Source note | uspto-grants-1989_06 |