Hydrochloric Acid → 1-Decyl-1,2,3,4-tetrahydro-8-quinolinol, hydrochloride

HRID 1905393Notes

Reaction equation

HRID 1905393 reaction equation
[CH2:1]([N:11]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][C:19]=2[OH:21])[CH2:14][CH2:13][CH2:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[ClH:22]>CCOCC>[ClH:22].[CH2:1]([N:11]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][C:19]=2[OH:21])[CH2:14][CH2:13][CH2:12]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 156313281-Decyl-1,2,3,4-tetrahydro-8-quinolinol

Product 1

HCID 156313291-Decyl-1,2,3,4-tetrahydro-8-quinolinol, hydrochloride

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

A solution of 575.9 mg (1.99 mmol) of 1-decyl-1,2,3,4-tetrahydro-8-quinolinol in 1 ml of ether was treated with 5 ml of hydrogen chloride-saturated ether to afford a soluble hydrochloride. Evaporation provided an oil which solidified upon standing to give 564.2 mg of a waxy, ivory-colored solid:melting point 82°-83° C.

Sources & evidence

ORD record
ord-a8f52b5a9aa54019941eb20543477382
Source dataset
uspto-grants-1989_06
Patent number
US04843082

Reaction notes

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