HRID1905393

反应详情

EQUATION

反应方程式

HRID 1905393 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 575.9 mg (1.99 mmol) of 1-decyl-1,2,3,4-tetrahydro-8-quinolinol in 1 ml of ether was treated with 5 ml of hydrogen chloride-saturated ether to afford a soluble hydrochloride. Evaporation provided an oil which solidified upon standing to give 564.2 mg of a waxy, ivory-colored solid:melting point 82°-83° C.