HRID1905440

反应详情

EQUATION

反应方程式

HRID 1905440 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

3 g (0.01 Mol) of 6-acetylamino-2-amino-4,5,6,7-tetrahydro-benzthiazole-hydrobromide are dissolved in 20 ml of semi-concentrated hydrobromic acid and refluxed for 6 hours. The solution is then concentrated by evaporation and the residue recrystallised from methanol.

WORKUP

后处理

  1. temperaturerefluxed for 6 hours
  2. concentrationThe solution is then concentrated by evaporation
  3. customthe residue recrystallised from methanol