HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 53778288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | O-ethylhydroxylamine hydrochloride | HCID 76850 | — |
| Reactant | HCID 20206284 | HCID 20206284 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 53778288 | HCID 53778288 | — |
Reaction Steps
Following the procedure of Example 1, 4-[4-(1-methylpropoxy)phenyl]-2-butanone (4.41 g, 20.0 mmol) and pyridine (3 ml) in 45 ml of tetrahydrofuran are reacted with ethoxyamine hydrochloride (4.41 g, 45.2 mmol) to give 4-[4-(1methylpropoxy)phenyl]-2-butanone O-ethyloxime, as a mixture of syn and anti stereo isomers. MS m/e 263 (M ).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04647698 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-2d3c3248b2c6452eb5efbe54b0209778 |
| Source note | uspto-grants-1987_03 |