Hydrogen Bromide → HCID 20213264, compound

HRID 1905865Notes

Reaction equation

HRID 1905865 reaction equation
[CH2:1]([N:3](C)[CH2:4][CH2:5][CH2:6]O)[CH3:2].[CH2:9]([NH:11][C:12]([NH:14][CH3:15])=[S:13])[CH3:10].Br>>[CH2:9]([NH:11][C:12](=[N:14][CH3:15])[S:13][CH2:6][CH2:5][CH2:4][NH:3][CH2:1][CH3:2])[CH3:10]

Participants

4

Reactant 3

HCID 260Hydrogen BromideHCID 144409693-[Ethyl(methyl)amino]propan-1-olHCID 15568242N-Ethyl-N'-methylthiourea

Product 1

HCID 20213264HCID 20213264, compound

Procedure

A mixture of 3-(ethylmethylamino)propanol, N-ethyl-N'-methylthiourea and aqueous hydrobromic acid is boiled under reflux to give the dihydrobromide salt of the title compound.

Workup

  1. temperatureunder reflux

Sources & evidence

ORD record
ord-d3d35a1a96ba475991b57b0eba5df0c0
Source dataset
uspto-grants-1987_03
Patent number
US04649138

Reaction notes

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