HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 20213386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 5,5-Diphenyl-2-thiohydantoin | HCID 854150 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20213386 | HCID 20213386 | 60% |
Reaction Steps
7.0 g of 5,5-diphenyl-2-thiohydantoin is dissolved in 50 ml of ethanol and 10 ml of 3N sodium carbonate added followed by 3 ml of iodomethane. The mixture is refluxed for 18 hours, then cooled and the solvent evaporated. The residual solid is recrystallized from ethanol to give 4.6 g (60%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649145 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-f98febb39d2045f1bff5d76a9b09caa6 |
| Source note | uspto-grants-1987_03 |