HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 13608180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 20213351 | HCID 20213351 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13608180 | HCID 13608180 | 93.7% |
Reaction Steps
To a solution of 3,4-dihydro-6-(3,4-methylenedioxyphenyl)-1-ethyl-3-methyl-4-(2,4,6-trimethylphenylimino)-2(1H)-pyrimidinone hydrochloride (70 mg) in water (10 ml) was neutralized with an aqueous solution of sodium bicarbonate. The resulting precipitates were collected by filtration to give 3,4-dihydro-6-(3,4-methylenedioxyphenyl)-1-ethyl-3-methyl-4-(2,4,6-trimethylphenylimino)-2(1H)-pyrimidinone (60 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649142 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-6dd07e88597348a7b89b911ba750606a |
| Source note | uspto-grants-1987_03 |