HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178432540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178474093 | HCID 178474093 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178432540 | HCID 178432540 | 77.8% |
Reaction Steps
A mixture of 2-methyl-4-(3-bromo-4-acetamido-phenyl)-1H-imidazole (15 g), concentrated hydrochloric acid (10 ml) and water (30 ml) was refluxed for 45 minutes. The resulting solution was cooled to room temperature and was made alkaline with 10% sodium hydroxide. The base was filtered off, washed with water and dried to give 10 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649150 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-7cf150e128504844842734ec82ff2680 |
| Source note | uspto-grants-1987_03 |