HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanimidic acid, N-cyano-, ethyl ester → HCID 178432550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanimidic acid, N-cyano-, ethyl ester | HCID 9920370 | — |
| Reactant | HCID 178432541 | HCID 178432541 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178432550 | HCID 178432550 | 77.9% |
Reaction Steps
A solution of 2-methyl-4-(4-amino-phenyl)-1H-imidazole (15 g) and ethyl N-cyanoformimidate (9.35 g) in ethanol (150 ml) was stirred at room temperature overnight. The product which crystallized out was collected by filtration, washed with cold ethanol and dried to give 15.2 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649150 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-65ce84783cb14901bddb68c68cc2adbc |
| Source note | uspto-grants-1987_03 |