Methylamine → HCID 178484895, compound

HRID 1905943Notes

Reaction equation

HRID 1905943 reaction equation
[C:1]([NH:3][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:13]=[C:14]([CH3:17])[NH:15][CH:16]=2)=[CH:8][CH:7]=1)#N.CN>>[CH3:1][NH:3][CH:4]=[N:5][C:6]1[CH:11]=[CH:10][C:9]([C:12]2[N:13]=[C:14]([CH3:17])[NH:15][CH:16]=2)=[CH:8][CH:7]=1

Participants

3

Reactant 2

HCID 6329MethylamineHCID 178432550HCID 178432550, compound

Product 1

HCID 178484895HCID 178484895, compoundYield 56.1%

Procedure

N-Cyano-N'-[4-(2-methyl-imidazol-4-yl)phenyl]-formamidine (2.25 g) was added all at once to a solution of methylamine 33% aqueous (22.5 ml). After a few minutes the solid which separated out was filtered off, washed with water and dried to give 1.2 g of the title compound.

Workup

  1. customAfter a few minutes the solid which separated out
  2. filtrationwas filtered off
  3. washwashed with water
  4. customdried

Sources & evidence

ORD record
ord-f5549676e5554f84a8e3f6ef545e8551
Source dataset
uspto-grants-1987_03
Patent number
US04649150

Reaction notes

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