HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13588837, compound → HCID 54395479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13588837 | HCID 13588837 | — |
| Solvent | Acetyl chloride | HCID 6367 | — |
| Product | HCID 54395479 | HCID 54395479 | 85% |
Reaction Steps
10 g of (5-isobutyl-2-thienyl)succinic acid was added to 40 cc of acetyl chloride and the mixture was refluxed for 1 hour 30 minutes. The excess acetyl chloride was evaporated under reduced pressure. Distillation of the residue provided 7.9 g (yield=85%) of (5-isobutyl-2-thienyl)succinic anhydride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649153 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-d99d16d11ac04b1e84b12f51b7d862ad |
| Source note | uspto-grants-1987_03 |