Methanesulfonyl chloride → 2-[2-(4-Methylthiophenyl)ethoxy]ethyl methanesulfonate
Reaction equation
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][O:11][CH2:12][CH2:13][OH:14])=[CH:5][CH:4]=1.[CH3:15][S:16](Cl)(=[O:18])=[O:17]>>[CH3:15][S:16]([O:14][CH2:13][CH2:12][O:11][CH2:10][CH2:9][C:6]1[CH:5]=[CH:4][C:3]([S:2][CH3:1])=[CH:8][CH:7]=1)(=[O:18])=[O:17]Participants
3
Procedure
The 2-[2-(4-methylthiophenyl)ethoxy]ethanol obtained according to the preceding paragraph was sulfonylated with methanesulfonyl chloride in a manner analogous to that described in Example 1(c) to give 2.41 g (90%) of 2-[2-(4-methylthiophenyl)ethoxy]ethyl methanesulfonate in the form of an oil which was homogeneous according to chromatography.
Sources & evidence
- ORD record
- ord-0a1b62e3dc3a46b3a8ca0372d8141c21
- Source dataset
- uspto-grants-1987_03
- Patent number
- US04649160
Reaction notes
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