HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → 2-[2-(4-Methylthiophenyl)ethoxy]ethyl methanesulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 2-[2-(4-Methylthiophenyl)ethoxy]ethanol | HCID 13208934 | — |
| Product | 2-[2-(4-Methylthiophenyl)ethoxy]ethyl methanesulfonate | HCID 13210824 | 90% |
Reaction Steps
The 2-[2-(4-methylthiophenyl)ethoxy]ethanol obtained according to the preceding paragraph was sulfonylated with methanesulfonyl chloride in a manner analogous to that described in Example 1(c) to give 2.41 g (90%) of 2-[2-(4-methylthiophenyl)ethoxy]ethyl methanesulfonate in the form of an oil which was homogeneous according to chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649160 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-0a1b62e3dc3a46b3a8ca0372d8141c21 |
| Source note | uspto-grants-1987_03 |