HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylglycerol tetrahydropyranyl ether → 3-(2-Hydroxyoctadecyloxy)-2-methoxypropyl tetrahydropyranyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylglycerol tetrahydropyranyl ether | HCID 13563077 | — |
| Reactant | 1,2-Epoxyoctadecene | HCID 20213826 | — |
| Product | 3-(2-Hydroxyoctadecyloxy)-2-methoxypropyl tetrahydropyranyl ether | HCID 20213824 | 55% |
Reaction Steps
The above 1,2-epoxyoctadecane (23) (5.5 g, 20.5 mmoles) was reacted with 7.8 g (41 mmoles) of 2-methylglycerol monotetrahydropyranyl ether in the same manner as Example 1-2 to give 5.1 g (55%) of the desired compound (24) as a colorless wax.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649203 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-72c28bc35aff4faaa6c01c8dc43e3823 |
| Source note | uspto-grants-1987_03 |