反应详情

In the manner described in Example 4, 101 g of triethylamine (1 mole) was dissolved in 200 g of polydimethylsiloxane. 137 g (1 mole) of benzyl chloride was stirred into this solution. After a reaction time of 5 hours at 80° C., a large amount of solid had formed, which was filtered out and washed with methyl ethyl ketone.

1. customAfter a reaction time of 5 hours at 80° C., a large amount of solid had formed
2. filtrationwhich was filtered out
3. washwashed with methyl ethyl ketone