Benzyl Chloride → Benzyl triethylammonium chloride

HRID 1906057Notes

Reaction equation

HRID 1906057 reaction equation
[CH2:1]([N:3]([CH2:6][CH3:7])[CH2:4][CH3:5])[CH3:2].[CH2:8]([Cl:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[Cl-:15].[CH2:8]([N+:3]([CH2:6][CH3:7])([CH2:4][CH3:5])[CH2:1][CH3:2])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 7503Benzyl ChlorideHCID 8471Triethylamine

Product 1

HCID 66133Benzyl triethylammonium chloride

Reagents, catalysts & solvents 1

HCID 178504327HCID 178504327, compoundSolvent

Procedure

In the manner described in Example 4, 101 g of triethylamine (1 mole) was dissolved in 200 g of polydimethylsiloxane. 137 g (1 mole) of benzyl chloride was stirred into this solution. After a reaction time of 5 hours at 80° C., a large amount of solid had formed, which was filtered out and washed with methyl ethyl ketone.

Workup

  1. customAfter a reaction time of 5 hours at 80° C., a large amount of solid had formed
  2. filtrationwhich was filtered out
  3. washwashed with methyl ethyl ketone

Sources & evidence

ORD record
ord-574ff3654bf44493ac0ae462a472faf9
Source dataset
uspto-grants-1987_03
Patent number
US04649220

Reaction notes

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