HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20213849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 19858589 | HCID 19858589 | — |
| Product | HCID 20213849 | HCID 20213849 | — |
Reaction Steps
10 g of methyl N-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenyl]-4-amino-n-butyrate (compound 2) are refluxed in 30 ml of acetyl chloride until the evolution of hydrogen chloride is complete. Excess acetyl chloride is removed in vacuo, affording the title compound in quantitative yield. nD21 =1.5437.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04649212 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-94ae5161d1bf4c19a222b377c8fb7699 |
| Source note | uspto-grants-1987_03 |