Sodium Carbonate → HCID 13827675, compound

HRID 1906064Notes

Reaction equation

HRID 1906064 reaction equation
[CH2:1]([NH:8][OH:9])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:10]1([CH2:18]Br)[CH:15]=[CH:14][C:13]([CH2:16]Br)=[CH:12][CH:11]=1.C(=O)([O-])[O-].[Na+].[Na+]>>[OH:9][N:8]([CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)[CH2:18][C:10]1[CH:15]=[CH:14][C:13]([CH2:16][N:8]([OH:9])[CH2:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[CH:12][CH:11]=1

Participants

4

Reactant 3

HCID 10340Sodium CarbonateHCID 693351,4-Bis(bromomethyl)benzeneHCID 2794173Benzylhydroxylamine

Product 1

HCID 13827675HCID 13827675, compound

Procedure

The procdure of Example 1 is repeated using 5.59 g of benzylhydroxylamine, 5.99 g of p-xylylene dibromide and 6.0 g of anhydrous sodium carbonate. The reaction product is recrystallized from acetonitrile to give the product as a white solid; m.p. 160°-163° C.

Workup

  1. customThe reaction product is recrystallized from acetonitrile

Sources & evidence

ORD record
ord-52111a3ec5fb4c96bd25605a70d3b7ea
Source dataset
uspto-grants-1987_03
Patent number
US04649221

Reaction notes

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