HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 2-(4-Nitrophenyl)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Methyl 2-(4-nitrophenyl)propionate | HCID 3016521 | — |
| Product | 2-(4-Nitrophenyl)propanamide | HCID 5086405 | — |
Reaction Steps
A solution of methyl 2-(4-nitrophenyl)propionate (20.0 g) in aqueous ammonia (d=0.88, 350 ml) was stirred at room temperature for 36 h. The resultant solid was collected and dried in vacuo at 50° to give the title compound (13.4 g). A sample (0.1 g) was crystallised from water to give analytically pure material m.p. 120°-121°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04650810 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-758bb40fb29d4230ac09c60e0033830c |
| Source note | uspto-grants-1987_03 |