HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminum(III) Chloride → HCID 57160591, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 20213089 | HCID 20213089 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | HCID 57160591 | HCID 57160591 | — |
Reaction Steps
This compound was prepared from 3-cyano-3,3-diphenyl-2-methyl-N,N-diisopropyl-propanamide, essentially as described in Example 6, but per mole of starting material are used 3 moles of LiAlH4 and 3 moles of AlCl3, and the amide is added slowly to the reducing agent under reflux and while stirring, whereupon the mixture was refluxed for 8-16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04650900 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-7fe4c0c141954a628bdfd1ee8c0894eb |
| Source note | uspto-grants-1987_03 |