O-ethylhydroxylamine hydrochloride → HCID 135974007, compound

Participants

Reaction Steps

Reaction of 3-hydroxy-5-(3-ethoxycarbonylthiocarbamoyl-2,4,6-trimethylphenyl)-2-propionylcyclohex-2-en-1-one with ethoxyamine hydrochloride following essentially the same procedure as that described in Example 1 part (v) gave 2-[1-(ethoxyimino)propyl]-3-hydroxy-5-(3-ethoxycarbonylthiocarbamoyl-2,4,6-trimethylphenyl)cyclohex-2-en-1-one (23) as a yellow oil. the compound was characterized by its proton nuclear magnetic resonance spectrum and the data are recorded in Table 3, Example 11.

Provenance & Evidence