HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-Amino-3-hydroxy-6-methyl-1-phenylheptane hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-t-Butyloxycarbonylamino-3-hydroxy-6-methyl-1-phenylheptane | HCID 13893153 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Amino-3-hydroxy-6-methyl-1-phenylheptane hydrochloride | HCID 20044148 | — |
Reaction Steps
The resultant compound of Example 1 (87 mg, 0.27 mmol) was dissolved in methanol (1 ml) and was treated with methanolic HCl (5 ml of 0.75M). After 15 hours the solution was evaporated to provide the desired compound as a glass (71 mg) which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04652551 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-906dd61b2f37435788b58d762f0e206a |
| Source note | uspto-grants-1987_03 |