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HRID1906642

反应详情

EQUATION

反应方程式

HRID 1906642 的结构方程式

REACTANTS

反应物

4
结构：O
HCID962

Water

H2O

结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：[K+].[OH-]
HCID14797

Potassium hydroxide

HKO

结构：CC(C=CC1C(C)(C)CCC1(C)C)NC(=O)OC(C)(C)C
HCID70445522

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(N)C=CC1C(C)(C)CCC1(C)C
HCID56622469

2-Amino-2-methyl-4-(2,2,5,5-tetramethyl-1-cyclopentyl)butene

C14H27N

PROCEDURE

实验过程

N-Boc-2-amino-4-(2,2,5,5-tetramethyl-1-cyclopentyl)-3-butene is dissolved in trifluoroacetic acid and the solution is stirred overnight. Water is added and the mixture is made basic with 20% KOH. The mixture is extracted with ether and the organic layer is dried over Na2SO4 and evaporated to yield 2-amino-2-methyl-4-(2,2,5,5-tetramethyl-1-cyclopentyl)butene.

WORKUP

后处理

  1. extractionThe mixture is extracted with ether
  2. dry with materialthe organic layer is dried over Na2SO4
  3. customevaporated