HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178461711, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178461710 | HCID 178461710 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178461711 | HCID 178461711 | — |
Reaction Steps
A solution of 0.87 g of hydrogen chloride in 20 ml of ethyl acetate was added dropwise at 5°, while stirring, to a solution of 3.1 g of p-[(S)-3-[(S)-2-phenyl-1-aziridinyl]butyl]benzamide in 150 ml of ethyl acetate. The precipitate was filtered off under suction and recrystallized from methanol/ether. There was obtained pure p-[(S)-3-[(S)-2-phenyl-1-aziridinyl]butyl]benzamide dihydrochloride of melting point 186°-188°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04652679 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-b8729e08ccdb4a63a061fae061a946ae |
| Source note | uspto-grants-1987_03 |