HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 20210822, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 2-(6,7-Dimethoxy-1,2,3,4-tetrahydro-isoquinolin-1-yl)-propane-1,3-diol | HCID 13696683 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20210822 | HCID 20210822 | — |
Reaction Steps
0.01 mole of 1-[bis(hydroxymethyl)-methyl]-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline is reacted with 0.03 mole of phenylisocyanate in toluene, as described in Example 22. The aimed compound is obtained, which has the same physical and analytical characteristics as the product of Example 26 (Table 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654351 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-d9efaae26a61442b9b18955a503bccda |
| Source note | uspto-grants-1987_03 |