1,1'-Carbonyldiimidazole → HCID 86739967, compound

HRID 1906754Notes

Reaction equation

HRID 1906754 reaction equation
[CH3:1][N:2]1[C:6]([C:7]([OH:9])=[O:8])=[CH:5][N:4]=[CH:3]1.C(N1C=CN=C1)(N1C=CN=C1)=O>C(Cl)Cl>[N-:2]1[CH:6]=[CH:5][N:4]=[CH:3]1.[CH3:1][N:2]1[C:6]([C:7]([OH:9])=[O:8])=[CH:5][N:4]=[CH:3]1

Participants

4

Reactant 2

HCID 682631,1'-CarbonyldiimidazoleHCID 27735071-methyl-1H-imidazole-5-carboxylic acid

Product 1

HCID 86739967HCID 86739967, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

1-methyl-5-imidazole carboxylic acid, 7.0 gm, was added to 50 ml of methylene chloride. 5.2 gm of carbonyldiimidazole was added to the system. The system was stirred at room temperature for 18 hours to give the 1-methyl-5-imidazolyl carboxylic acid imidazolide.

Sources & evidence

ORD record
ord-dd56fd03bef9490ba95cb44b82b1fffa
Source dataset
uspto-grants-1987_03
Patent number
US04654346

Reaction notes

Loading…