HuagongsheHuagongshe Chemistry Print Report · For research reference only
3'-Aminoacetophenone → HCID 898301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3'-Aminoacetophenone | HCID 7417 | — |
| Reactant | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 898301 | HCID 898301 | — |
Reaction Steps
An 11.4 g portion of m-aminoacetophenone, 10.9 g of diisopropylethylamine, 10.0 g of cyclobutanecarboxylic acid chloride and 200 ml of dichloromethane were reacted as described in Example 1, giving 14.68 g of N-(3-acetylphenyl)cyclobutanecarboxamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654347 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-b2c806a863084c318dacd8fdd1be75b6 |
| Source note | uspto-grants-1987_03 |