HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → Carbamic acid, (3-acetylphenyl)-, methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | 3'-Aminoacetophenone | HCID 7417 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Carbamic acid, (3-acetylphenyl)-, methyl ester | HCID 4049280 | — |
Reaction Steps
A mixture of m-aminoacetophenone, diisopropylethylamine, methyl chloroformate and dichloromethane was reacted as described in Example 1, giving 33.4 g of (3-acetylphenyl)carbamic acid, methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654347 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-4e7b9e104ff64fef9644544b8c32a0e3 |
| Source note | uspto-grants-1987_03 |