HuagongsheHuagongshe Chemistry Print Report · For research reference only
3'-Aminoacetophenone → HCID 1640925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3'-Aminoacetophenone | HCID 7417 | — |
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 1640925 | HCID 1640925 | 89.5% |
Reaction Steps
A mixture of 27.03 g of m-aminoacetophenone, 25.85 g of diisopropylethylamine, 27.32 g of n-butyl chloroformate and 300 ml of dichloromethane was reacted as described in Example 1, giving 42.10 g of (3-acetylphenyl)carbamic acid, butyl ester, mp 59°-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654347 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-4664e600bde543f389f970903dc58eb2 |
| Source note | uspto-grants-1987_03 |