HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 20210647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 13824243 | HCID 13824243 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20210647 | HCID 20210647 | — |
Reaction Steps
As described for Example 59, 0.01 mole of N-[3-(3-benzoylpyrazolo[1,5-a]pyrimidin-7-yl]phenyl]formamide in 30 ml of dimethylformamide is reacted with 0.384 g of 60% sodium hydride in oil. To the mixture is added 0.85 ml of ethyl iodide and the mixture stirred overnight. Work up as for Example 59 gives the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654347 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-3a74657925dc4d70b7185fe0c0da5c86 |
| Source note | uspto-grants-1987_03 |