HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-(chloromethyl)benzene → HCID 13800177, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-(chloromethyl)benzene | HCID 7723 | — |
| Reactant | HCID 13442942 | HCID 13442942 | — |
| Product | HCID 13800177 | HCID 13800177 | — |
Reaction Steps
This compound was prepared in the same manner as described in Example 17 except that following the addition of 4-chlorobenzylchloride to the anion of 2-chloro-3-phenylsulfonylindole, the reaction mixture was stirred at 90° for 4 hours. The crude product was crystallized from dichloromethane-hexane to give the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654360 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-b275bd167382440d8f8733643d917164 |
| Source note | uspto-grants-1987_03 |