HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → 1-(4-Carbobenzyloxyphenyl)propan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 4-(2-Oxopropyl)benzoyl chloride | HCID 20134178 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 1-(4-Carbobenzyloxyphenyl)propan-2-one | HCID 20134244 | — |
Reaction Steps
4-Acetonylbenzoyl chloride (3.92 g) and benzyl alcohol (2.16 g) were refluxed in benzene for 4 hours and then left at room temperature for 48 hours. Removal of the solvent gave the title compound. τ (CDCl3) 7.9 (3H, s), 6.32 (2H, s), 4.69 (2H, s), 2.78 (2H, d, J=8 Hz), 2.70 (5H, m), 1.99 (2H, d, J=8 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04654371 |
| Source dataset | uspto-grants-1987_03 |
| ORD ID | ord-2db79194f9a0468fafca77f60109b1f9 |
| Source note | uspto-grants-1987_03 |