HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178492052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 178492053 | HCID 178492053 | — |
| Reactant | HCID 178515224 | HCID 178515224 | — |
| Product | HCID 178492052 | HCID 178492052 | — |
Reaction Steps
The title compound was prepared following the procedure for 14a using 13c and 1-methylpiperazine. 1H-NMR (CD3OD) δ (ppm): 2.32 (3H, s), 2.67 (4H, brm), 3.40 (4H, brm), 3.85 (3H, s), 6.88 (2H, m), 7.02 (1H, d, J=2.47 Hz), 7.31 (1H, dd, J=9.06, 2.20 Hz), 7.66 (2H, m), 8.16 (1H, d, J=9.06 Hz), 8.52 (1H, s). m/z 390.4 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598159B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-ef7e02b579564571a291e1947a0b045e |
| Source note | uspto-grants-2013_12 |