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HRID1907482

反应详情

EQUATION

反应方程式

HRID 1907482 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])c1ccc(N2CCNCC2)cc1
HCID80447

1-(4-Nitrophenyl)piperazine

C10H13N3O2

结构：CCOC(=O)Nc1nc2cc(Cl)ccc2nc1OC
HCID66918182

未命名化合物

PRODUCTS

生成物

1
结构：COc1nc2ccc(Cl)cc2nc1NC(=O)N1CCN(c2ccc([N+](=O)[O-])cc2)CC1
HCID66918087

未命名化合物

收率 82%

PROCEDURE

实验过程

Ethyl N-(6-chloro-2-methoxyquinoxalin-3-yl)carbamate and 1-(4-nitrophenyl)piperazine were reacted by the same way with the example 22 to obtain the titled compound (yield, 82%). 1H NMR (300 MHz, DMSO-d6): δ 3.62-3.66 (m, 8H), 4.06 (s, 3H), 7.07 (d, J=9.0 Hz, 2H), 7.58 (d, J=8.4 Hz, 1H), 7.76-7.80 (m, 2H), 8.11 (d, J=9.0 Hz, 2H), 9.46 (s, 1H).