HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazin-4-ylacetophenone → HCID 69242445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazin-4-ylacetophenone | HCID 97269 | — |
| Reactant | ethyl N-(6-fluoro-3-methoxyquinoxalin-2-yl)carbamate | HCID 69243333 | — |
| Product | HCID 69242445 | HCID 69242445 | 91% |
Reaction Steps
Ethyl N-(6-fluoro-3-methoxyquinoxalin-2-yl)carbamate and 1-(4-acetylphenyl)piperazine were reacted by the same way with the example 85 to obtain the titled compound (yield, 91%). 1H NMR (200 MHz, CDCl3): δ 2.54 (s, 3H), 3.50 (s, 4H), 3.90 (s, 4H), 4.15 (s, 3H), 6.89 (d, J=8.7 Hz, 2H), 7.25-7.62 (m, 3H), 7.79 (s, 1H), 7.91 (d, J=9.0 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-14c6d20ead634279abf0f6d6cbb7f0d6 |
| Source note | uspto-grants-2013_12 |