HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Pyridyl)piperazine → HCID 69245226, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Pyridyl)piperazine | HCID 94459 | — |
| Reactant | ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate | HCID 69243736 | — |
| Product | HCID 69245226 | HCID 69245226 | 88% |
Reaction Steps
Ethyl N-(3-methoxy-6-methylquinoxalin-2-yl)carbamate and 1-(2-pyridyl)piperazine were reacted by the same way with the example 127 to obtain the titled compound (yield, 88%). 1H NMR (300 MHz, CDCl3): δ 2.49 (s, 3H), 3.61-3.71 (m, 8H), 4.12 (s, 3H), 6.66 (d, J=8 Hz, 2H), 7.07-7.74 (m, 5H), 8.20 (dd, J=5.4, 1.8 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-144bc944ed554064965fc98fd452c1f2 |
| Source note | uspto-grants-2013_12 |