HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Cyanophenyl)piperazine → HCID 69244372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Cyanophenyl)piperazine | HCID 2735875 | — |
| Reactant | ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate | HCID 69244324 | — |
| Product | HCID 69244372 | HCID 69244372 | 97% |
Reaction Steps
Ethyl N-(3,6-dimethoxyquinoxalin-2-yl)carbamate and 1-(2-cyanophenyl)piperazine were reacted by the same way with the example 148 to obtain the titled compound (yield, 97%). 1H NMR (300 MHz, CDCl3): δ 2.46 (s, 3H), 3.28 (s, 4H), 3.86 (s, 3H), 4.08-4.19 (m, 4H), 7.01-7.08 (m, 3H), 7.17-7.37 (m, 1H), 7.49-7.61 (m, 4H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-5d86923e54804b6a91433986a7eebfa4 |
| Source note | uspto-grants-2013_12 |