HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromophenyl)piperazine → HCID 69241684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromophenyl)piperazine | HCID 2757154 | — |
| Reactant | Ethyl N-(2,6,7-trimethoxyquinoxalin-3-yl)carbamate | HCID 69244380 | — |
| Product | HCID 69241684 | HCID 69241684 | 63% |
Reaction Steps
Ethyl N-(2,6,7-trimethoxyquinoxalin-3-yl)carbamate and 1-(3-bromophenyl) piperazine were reacted by the same way with the example 190 to obtain the titled compound (yield, 63%) H NMR (300 MHz, CDCl3) δ 3.28-3.30 (m, 4H), 3.78 (m, 4H), 3.97 (s, 3H), 3.99 (s, 3H), 4.13 (s, 3H), 6.86 (m, 1H), 7.01 (s, 1H), 7.06-7.07 (m, 1H), 7.13-7.16 (m, 2H), 7.22-7.28 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598173B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-b85f88bd79db45c0a15aa97c773f1462 |
| Source note | uspto-grants-2013_12 |