HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 69100806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 59737532 | HCID 59737532 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69100806 | HCID 69100806 | 46% |
Reaction Steps
Following the same procedure as described in Example 14, step 4 (scheme 14) but substituting compound 146 for compound 192, the title compound 193 was obtained after column chromatography (46% yield, eluent: 50% MeOH in DCM with 1% triethylamine).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598168B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-288223e7287d48408c77e89d0fb7be07 |
| Source note | uspto-grants-2013_12 |