HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 59737296, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 59737457 | HCID 59737457 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59737296 | HCID 59737296 | 90% |
Reaction Steps
Following the same procedure as described in Example 20, step 5 (scheme 20) but substituting compound 189 for compound 198, title compound 199 was obtained in 90% yield [after column chromatography (eluent: 25% AcOEt in DCM)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598168B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-0f70abb40f92493fa893d7473f3311c3 |
| Source note | uspto-grants-2013_12 |