HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 59737349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 59737478 | HCID 59737478 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59737349 | HCID 59737349 | 92% |
Reaction Steps
A suspension of acetate 296 (349 mg, 0.99 mmol) in dry MeOH (6 mL) was treated with triethyl amine (1.5 mL) and stirred at room temperature for 19 h, concentrated under reduced pressure and triturated with diethyl ether to provide the title compound 297 (282.5 mg, 92% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598168B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-6a5ce18d6ab84384ab55bd46ea2aa3a4 |
| Source note | uspto-grants-2013_12 |