HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-methoxy-6-methyl-4-nitropyridazine 1-oxide → HCID 21766149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-methoxy-6-methyl-4-nitropyridazine 1-oxide | HCID 6405305 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21766149 | HCID 21766149 | — |
Reaction Steps
3-Methoxy-6-methyl-4-nitropyridazine 1-oxide (1 g) was converted and worked up analogously to example 1 g). Chromatography of the crude product was unnecessary. The solvent used was methanol (30 ml), and the base sodium methoxide (as 30% solution in methanol, 1.1 ml). Yield: 900 mg LC-MS Rt: 0.29 min [M+H]+:171.1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598177B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-73fa67287c55470cb6a518fcc5adc71e |
| Source note | uspto-grants-2013_12 |