HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66997917, compound → HCID 66997919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66997917 | HCID 66997917 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66997919 | HCID 66997919 | — |
Reaction Steps
The product obtained in 83c (100 mg, 0.34 mmol) in 10 mL methanol was mixed with Raney nickel (25 mg) and hydrogenated at 3.4 bar for 2.5 h in a Parr apparatus. The mixture was filtered and the filtrate concentrated i. vac.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598190B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-36a3cf9162934be5910aebb7bc371a70 |
| Source note | uspto-grants-2013_12 |