HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-amino-5-nitropyridine-2-carboxylate → Methyl 4,5-diaminopicolinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-amino-5-nitropyridine-2-carboxylate | HCID 46835478 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Methyl 4,5-diaminopicolinate | HCID 66997018 | — |
Reaction Steps
Prepared analogously to example 83d by hydrogenation of methyl-4-amino-5-nitropicolinate using palladium/charcoal 10% in THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598190B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-27962eb3ad594589bff808d237e2923a |
| Source note | uspto-grants-2013_12 |