HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorobenzene → HCID 15366480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorobenzene | HCID 7964 | — |
| Reactant | Homophthalic anhydride | HCID 12801 | — |
| Product | HCID 15366480 | HCID 15366480 | — |
Reaction Steps
2-[2-(4-Chlorophenyl)-2-oxoethyl]-benzoic acid (above) was prepared by method I using homophthalic anhydride and chlorobenzene. In this case, it was found to be advantageous to heat the reaction to 85° C. for 4 hours. The product was isolated by flash chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08598194B2 |
| Source dataset | uspto-grants-2013_12 |
| ORD ID | ord-b1e6797c1f554ad7b381c25036c973a4 |
| Source note | uspto-grants-2013_12 |