Cyclohexanone → HCID 16682041, compound

Participants

Reaction Steps

The title compound was prepared using the procedure as described in Example 1A, substituting 2′-hydroxy-5′-methylacetophenone (Aldrich, CAS#1450-72-2) for 2′-hydroxyacetophenone and cyclopentanone for cyclohexanone. 1H NMR (300 MHz, DMSO-d6) δ ppm 7.51 (m, 1H), 7.35 (m, 1H), 6.87 (d, J=8.5 Hz, 1H), 2.85 (s, 2H), 2.26 (s, 3H), 1.89-1.95 (m, 2H), 1.59-1.79 (m, 6H). MS (DCI+) m/z 217 (M+H), 234 (M+NH4).

Provenance & Evidence